A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

Rachel J. Husband; Cornelius Strohm; Karen Appel; Orianna B. Ball; Richard Briggs; Johannes Buchen; Valerio Cerantola; Stella Chariton; Amy L. Coleman; Hyunchae Cynn; Dana Dattelbaum; Anand Dwivedi; Jon H. Eggert; Lars Ehm; William J. Evans; Konstantin Glazyrin; Alexander F. Goncharov; Heinz Graafsma; Alex Howard; Larissa Huston; Trevor M. Hutchinson; Huijeong Hwang; Sony Jacob; Johannes Kaa; Jaeyong Kim; Minseob Kim; Egor Koemets; Zuzana Konôpková; Falko Langenhorst; Torsten Laurus; Xinyang Li; Jona Mainberger; Hauke Marquardt; Emma E. Mcbride; Christopher Mcguire; James D. Mchardy; Malcolm I. Mcmahon; R. Stewart Mcwilliams; Alba S.J. Méndez; Anshuman Mondal; Guillaume Morard; Earl F. O'bannon; Christoph Otzen; Charles M. Pépin; Vitali B. Prakapenka; Clemens Prescher; Thomas R. Preston; Ronald Redmer; Michael Roeper; Carmen Sanchez-Valle; Dean Smith; Raymond F. Smith; Daniel Sneed; Sergio Speziale; Tobias Spitzbart; Stephan Stern; Blake T. Sturtevant; Jolanta Sztuk-Dambietz; Peter Talkovski; Nenad Velisavljevic; Cara Vennari; Zhongyan Wu; Choong Shik Yoo; Ulf Zastrau; Zsolt Jenei; Hanns Peter Liermann

doi:10.1107/S1600577523003910

A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

Rachel J. Husband^*, Cornelius Strohm, Karen Appel, Orianna B. Ball, Richard Briggs, Johannes Buchen, Valerio Cerantola, Stella Chariton, Amy L. Coleman, Hyunchae Cynn, Dana Dattelbaum, Anand Dwivedi, Jon H. Eggert, Lars Ehm, William J. Evans, Konstantin Glazyrin, Alexander F. Goncharov, Heinz Graafsma, Alex Howard, Larissa HustonTrevor M. Hutchinson, Huijeong Hwang, Sony Jacob, Johannes Kaa, Jaeyong Kim, Minseob Kim, Egor Koemets, Zuzana Konôpková, Falko Langenhorst, Torsten Laurus, Xinyang Li, Jona Mainberger, Hauke Marquardt, Emma E. Mcbride, Christopher Mcguire, James D. Mchardy, Malcolm I. Mcmahon, R. Stewart Mcwilliams, Alba S.J. Méndez, Anshuman Mondal, Guillaume Morard, Earl F. O'bannon, Christoph Otzen, Charles M. Pépin, Vitali B. Prakapenka, Clemens Prescher, Thomas R. Preston, Ronald Redmer, Michael Roeper, Carmen Sanchez-Valle, Dean Smith, Raymond F. Smith, Daniel Sneed, Sergio Speziale, Tobias Spitzbart, Stephan Stern, Blake T. Sturtevant, Jolanta Sztuk-Dambietz, Peter Talkovski, Nenad Velisavljevic, Cara Vennari, Zhongyan Wu, Choong Shik Yoo, Ulf Zastrau, Zsolt Jenei, Hanns Peter Liermann^*

^*Corresponding author for this work

School of Mathematics and Physics

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Abstract

An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤10³ s⁻¹), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s⁻¹ was observed during the fast compression of Au, while a strain rate of ∼1100 s⁻¹ was achieved during the rapid compression of N₂ at 23 TPa s⁻¹.

Original language	English
Pages (from-to)	671-685
Number of pages	15
Journal	Journal of Synchrotron Radiation
Volume	30
DOIs	https://doi.org/10.1107/S1600577523003910
Publication status	Published - 15 Jun 2023

Keywords

diamond anvil cells
dynamic compression
extreme conditions science
X-ray free-electron lasers

ASJC Scopus subject areas

Radiation
Nuclear and High Energy Physics
Instrumentation

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10.1107/S1600577523003910Licence: CC BY

A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell
Copyright 2023 The Authors. This is an open access article published under a Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium, provided the author and source are cited.
Final published version, 1.92 MBLicence: CC BY

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Husband, R. J., Strohm, C., Appel, K., Ball, O. B., Briggs, R., Buchen, J., Cerantola, V., Chariton, S., Coleman, A. L., Cynn, H., Dattelbaum, D., Dwivedi, A., Eggert, J. H., Ehm, L., Evans, W. J., Glazyrin, K., Goncharov, A. F., Graafsma, H., Howard, A., ... Liermann, H. P. (2023). A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell. Journal of Synchrotron Radiation, 30, 671-685. https://doi.org/10.1107/S1600577523003910

@article{058b0d841d49462a8b093043dec3a954,

title = "A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell",

abstract = "An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.",

keywords = "diamond anvil cells, dynamic compression, extreme conditions science, X-ray free-electron lasers",

author = "Husband, {Rachel J.} and Cornelius Strohm and Karen Appel and Ball, {Orianna B.} and Richard Briggs and Johannes Buchen and Valerio Cerantola and Stella Chariton and Coleman, {Amy L.} and Hyunchae Cynn and Dana Dattelbaum and Anand Dwivedi and Eggert, {Jon H.} and Lars Ehm and Evans, {William J.} and Konstantin Glazyrin and Goncharov, {Alexander F.} and Heinz Graafsma and Alex Howard and Larissa Huston and Hutchinson, {Trevor M.} and Huijeong Hwang and Sony Jacob and Johannes Kaa and Jaeyong Kim and Minseob Kim and Egor Koemets and Zuzana Kon{\^o}pkov{\'a} and Falko Langenhorst and Torsten Laurus and Xinyang Li and Jona Mainberger and Hauke Marquardt and Mcbride, {Emma E.} and Christopher Mcguire and Mchardy, {James D.} and Mcmahon, {Malcolm I.} and Mcwilliams, {R. Stewart} and M{\'e}ndez, {Alba S.J.} and Anshuman Mondal and Guillaume Morard and O'bannon, {Earl F.} and Christoph Otzen and P{\'e}pin, {Charles M.} and Prakapenka, {Vitali B.} and Clemens Prescher and Preston, {Thomas R.} and Ronald Redmer and Michael Roeper and Carmen Sanchez-Valle and Dean Smith and Smith, {Raymond F.} and Daniel Sneed and Sergio Speziale and Tobias Spitzbart and Stephan Stern and Sturtevant, {Blake T.} and Jolanta Sztuk-Dambietz and Peter Talkovski and Nenad Velisavljevic and Cara Vennari and Zhongyan Wu and Yoo, {Choong Shik} and Ulf Zastrau and Zsolt Jenei and Liermann, {Hanns Peter}",

year = "2023",

month = jun,

day = "15",

doi = "10.1107/S1600577523003910",

language = "English",

volume = "30",

pages = "671--685",

journal = "Journal of Synchrotron Radiation",

issn = "0909-0495",

publisher = "International Union of Crystallography",

}

Husband, RJ, Strohm, C, Appel, K, Ball, OB, Briggs, R, Buchen, J, Cerantola, V, Chariton, S, Coleman, AL, Cynn, H, Dattelbaum, D, Dwivedi, A, Eggert, JH, Ehm, L, Evans, WJ, Glazyrin, K, Goncharov, AF, Graafsma, H, Howard, A, Huston, L, Hutchinson, TM, Hwang, H, Jacob, S, Kaa, J, Kim, J, Kim, M, Koemets, E, Konôpková, Z, Langenhorst, F, Laurus, T, Li, X, Mainberger, J, Marquardt, H, Mcbride, EE, Mcguire, C, Mchardy, JD, Mcmahon, MI, Mcwilliams, RS, Méndez, ASJ, Mondal, A, Morard, G, O'bannon, EF, Otzen, C, Pépin, CM, Prakapenka, VB, Prescher, C, Preston, TR, Redmer, R, Roeper, M, Sanchez-Valle, C, Smith, D, Smith, RF, Sneed, D, Speziale, S, Spitzbart, T, Stern, S, Sturtevant, BT, Sztuk-Dambietz, J, Talkovski, P, Velisavljevic, N, Vennari, C, Wu, Z, Yoo, CS, Zastrau, U, Jenei, Z & Liermann, HP 2023, 'A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell', Journal of Synchrotron Radiation, vol. 30, pp. 671-685. https://doi.org/10.1107/S1600577523003910

TY - JOUR

T1 - A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

AU - Husband, Rachel J.

AU - Strohm, Cornelius

AU - Appel, Karen

AU - Ball, Orianna B.

AU - Briggs, Richard

AU - Buchen, Johannes

AU - Cerantola, Valerio

AU - Chariton, Stella

AU - Coleman, Amy L.

AU - Cynn, Hyunchae

AU - Dattelbaum, Dana

AU - Dwivedi, Anand

AU - Eggert, Jon H.

AU - Ehm, Lars

AU - Evans, William J.

AU - Glazyrin, Konstantin

AU - Goncharov, Alexander F.

AU - Graafsma, Heinz

AU - Howard, Alex

AU - Huston, Larissa

AU - Hutchinson, Trevor M.

AU - Hwang, Huijeong

AU - Jacob, Sony

AU - Kaa, Johannes

AU - Kim, Jaeyong

AU - Kim, Minseob

AU - Koemets, Egor

AU - Konôpková, Zuzana

AU - Langenhorst, Falko

AU - Laurus, Torsten

AU - Li, Xinyang

AU - Mainberger, Jona

AU - Marquardt, Hauke

AU - Mcbride, Emma E.

AU - Mcguire, Christopher

AU - Mchardy, James D.

AU - Mcmahon, Malcolm I.

AU - Mcwilliams, R. Stewart

AU - Méndez, Alba S.J.

AU - Mondal, Anshuman

AU - Morard, Guillaume

AU - O'bannon, Earl F.

AU - Otzen, Christoph

AU - Pépin, Charles M.

AU - Prakapenka, Vitali B.

AU - Prescher, Clemens

AU - Preston, Thomas R.

AU - Redmer, Ronald

AU - Roeper, Michael

AU - Sanchez-Valle, Carmen

AU - Smith, Dean

AU - Smith, Raymond F.

AU - Sneed, Daniel

AU - Speziale, Sergio

AU - Spitzbart, Tobias

AU - Stern, Stephan

AU - Sturtevant, Blake T.

AU - Sztuk-Dambietz, Jolanta

AU - Talkovski, Peter

AU - Velisavljevic, Nenad

AU - Vennari, Cara

AU - Wu, Zhongyan

AU - Yoo, Choong Shik

AU - Zastrau, Ulf

AU - Jenei, Zsolt

AU - Liermann, Hanns Peter

PY - 2023/6/15

Y1 - 2023/6/15

N2 - An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.

AB - An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.

KW - diamond anvil cells

KW - dynamic compression

KW - extreme conditions science

KW - X-ray free-electron lasers

U2 - 10.1107/S1600577523003910

DO - 10.1107/S1600577523003910

M3 - Article

C2 - 37318367

AN - SCOPUS:85164252671

SN - 0909-0495

VL - 30

SP - 671

EP - 685

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

ER -

A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

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Keywords

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