Abstract
A novel route involving atmospheric pressure chemical vapour deposition (APCVD) is reported for coating Nb2O5 onto glass substrates via the reaction of NbCl5 and ethyl acetate at 400-660degreesC. Raman spectroscopy is shown to be a simple diagnostic tool for the analysis of these thin films. The contact angle of water on Nb2O5-coated glass drops on UV irradiation from 60degrees to 5-20degrees. XPS Analysis showed that the Nb:O ratio of the film was 1:2.5. Glancing angle X-ray diffraction showed that all films were crystalline, with only a single phase being observed; this has some preferred orientation in the (201) plane of Nb2O5. The niobium(V) oxide materials show minimal photocatalytic ability to degrade organic material.
| Original language | English |
|---|---|
| Pages (from-to) | 2952-2956 |
| Number of pages | 5 |
| Journal | Journal of Materials Chemistry |
| Volume | 13 |
| Issue number | 12 |
| DOIs | |
| Publication status | Published - Dec 2003 |
ASJC Scopus subject areas
- Physical and Theoretical Chemistry
- Materials Chemistry
- Materials Science(all)