Conserved hydrogen bonding in tetrahydrocarbazolone derivatives: influence of solution-state assembly on crystal form nucleation

Robert M. Edkins, Elliott Hayden, Jonathan W. Steed, Katharina Edkins

Research output: Contribution to journalArticlepeer-review

5 Citations (Scopus)
286 Downloads (Pure)

Abstract

Two tetrahydocarbazolone derivatives were found to show multiple unsolvated crystal forms. A persistent dimer motif was detected in solution by FTIR spectroscopy that is maintained in the kinetic crystal forms. Rationally introduced steric bulk induces the formation of a more stable catemeric form.
Original languageEnglish
Pages (from-to)5314-5317
JournalChemical Communications
Volume51
Issue number25
Early online date17 Feb 2015
DOIs
Publication statusPublished - 2015

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