DON calibrant: Towards the production of certified B-trichothecene calibrants

A. Parich; H. Pettersson; R. D. Josephs; H. P. Van Egmond; R. Schothorst; P. Brereton; D. Chan; R. Krska

doi:10.1007/BF02954805

DON calibrant: Towards the production of certified B-trichothecene calibrants

A. Parich^*
, H. Pettersson
, R. D. Josephs
, H. P. Van Egmond
, R. Schothorst
, P. Brereton
, D. Chan
, R. Krska

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

Within an EC-funded project calibrants with certified concentrations of Deoxynivalenol (DON), 3-Acetyl-Deoxynivalenol (3-Ac-DON), 15-Acetyl- Deoxynivalenol (15-Ac-DON) and Nivalenol (NTV) in acetonitrile have been produced. So far the project has led to improved isolation and purification of the solid toxins from Fusarium cultures. In addition, conditions for the production, ampouling and transport of the toxin solutions have been optimised. Further investigations should lead to knowledge about storage conditions and internationally accepted molar absorption coefficients for DON, 3-Ac-DON, 15-Ac-DON and NIV in acetonitrile. The intercomparison study which is currently carried out will also help to support knowledge and experience exchange between laboratories in the field of Fusarium mycotoxin analysis.

Original language	English
Pages (from-to)	7-10
Number of pages	4
Journal	Mycotoxin Research
Volume	21
Issue number	1
DOIs	https://doi.org/10.1007/BF02954805
Publication status	Published - 01 Mar 2005
Externally published	Yes

Keywords

B-trichothecenes
Certified calibrants
Deoxynivalenol

ASJC Scopus subject areas

Microbiology
Toxicology
Biotechnology

Access to Document

10.1007/BF02954805

Cite this

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title = "DON calibrant: Towards the production of certified B-trichothecene calibrants",

abstract = "Within an EC-funded project calibrants with certified concentrations of Deoxynivalenol (DON), 3-Acetyl-Deoxynivalenol (3-Ac-DON), 15-Acetyl- Deoxynivalenol (15-Ac-DON) and Nivalenol (NTV) in acetonitrile have been produced. So far the project has led to improved isolation and purification of the solid toxins from Fusarium cultures. In addition, conditions for the production, ampouling and transport of the toxin solutions have been optimised. Further investigations should lead to knowledge about storage conditions and internationally accepted molar absorption coefficients for DON, 3-Ac-DON, 15-Ac-DON and NIV in acetonitrile. The intercomparison study which is currently carried out will also help to support knowledge and experience exchange between laboratories in the field of Fusarium mycotoxin analysis.",

keywords = "B-trichothecenes, Certified calibrants, Deoxynivalenol",

author = "A. Parich and H. Pettersson and Josephs, \{R. D.\} and \{Van Egmond\}, \{H. P.\} and R. Schothorst and P. Brereton and D. Chan and R. Krska",

year = "2005",

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day = "1",

doi = "10.1007/BF02954805",

language = "English",

volume = "21",

pages = "7--10",

journal = "Mycotoxin Research",

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publisher = "Springer Science and Business Media Deutschland GmbH",

number = "1",

}

TY - JOUR

T1 - DON calibrant

T2 - Towards the production of certified B-trichothecene calibrants

AU - Parich, A.

AU - Pettersson, H.

AU - Josephs, R. D.

AU - Van Egmond, H. P.

AU - Schothorst, R.

AU - Brereton, P.

AU - Chan, D.

AU - Krska, R.

PY - 2005/3/1

Y1 - 2005/3/1

N2 - Within an EC-funded project calibrants with certified concentrations of Deoxynivalenol (DON), 3-Acetyl-Deoxynivalenol (3-Ac-DON), 15-Acetyl- Deoxynivalenol (15-Ac-DON) and Nivalenol (NTV) in acetonitrile have been produced. So far the project has led to improved isolation and purification of the solid toxins from Fusarium cultures. In addition, conditions for the production, ampouling and transport of the toxin solutions have been optimised. Further investigations should lead to knowledge about storage conditions and internationally accepted molar absorption coefficients for DON, 3-Ac-DON, 15-Ac-DON and NIV in acetonitrile. The intercomparison study which is currently carried out will also help to support knowledge and experience exchange between laboratories in the field of Fusarium mycotoxin analysis.

AB - Within an EC-funded project calibrants with certified concentrations of Deoxynivalenol (DON), 3-Acetyl-Deoxynivalenol (3-Ac-DON), 15-Acetyl- Deoxynivalenol (15-Ac-DON) and Nivalenol (NTV) in acetonitrile have been produced. So far the project has led to improved isolation and purification of the solid toxins from Fusarium cultures. In addition, conditions for the production, ampouling and transport of the toxin solutions have been optimised. Further investigations should lead to knowledge about storage conditions and internationally accepted molar absorption coefficients for DON, 3-Ac-DON, 15-Ac-DON and NIV in acetonitrile. The intercomparison study which is currently carried out will also help to support knowledge and experience exchange between laboratories in the field of Fusarium mycotoxin analysis.

KW - B-trichothecenes

KW - Certified calibrants

KW - Deoxynivalenol

UR - https://www.scopus.com/pages/publications/84898758208

U2 - 10.1007/BF02954805

DO - 10.1007/BF02954805

M3 - Article

AN - SCOPUS:84898758208

SN - 0178-7888

VL - 21

SP - 7

EP - 10

JO - Mycotoxin Research

JF - Mycotoxin Research

IS - 1

ER -

DON calibrant: Towards the production of certified B-trichothecene calibrants

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

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