High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser

L. Wollenweber; T. R. Preston; A. Descamps; V. Cerantola; A. Comley; J. H. Eggert; L. B. Fletcher; G. Geloni; D. O. Gericke; S. H. Glenzer; S. Göde; J. Hastings; O. S. Humphries; A. Jenei; O. Karnbach; Z. Konopkova; R. Loetzsch; B. Marx-Glowna; E. E. McBride; D. McGonegle; G. Monaco; B. K. Ofori-Okai; C. A.J. Palmer; C. Plückthun; R. Redmer; C. Strohm; I. Thorpe; T. Tschentscher; I. Uschmann; J. S. Wark; T. G. White; K. Appel; G. Gregori; U. Zastrau

doi:10.1063/5.0022886

High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser

L. Wollenweber^*, T. R. Preston, A. Descamps, V. Cerantola, A. Comley, J. H. Eggert, L. B. Fletcher, G. Geloni, D. O. Gericke, S. H. Glenzer, S. Göde, J. Hastings, O. S. Humphries, A. Jenei, O. Karnbach, Z. Konopkova, R. Loetzsch, B. Marx-Glowna, E. E. McBride, D. McGonegleG. Monaco, B. K. Ofori-Okai, C. A.J. Palmer, C. Plückthun, R. Redmer, C. Strohm, I. Thorpe, T. Tschentscher, I. Uschmann, J. S. Wark, T. G. White, K. Appel, G. Gregori, U. Zastrau

^*Corresponding author for this work

School of Mathematics and Physics

Research output: Contribution to journal › Article › peer-review

26 Citations (Scopus)

97 Downloads (Pure)

Abstract

We introduce a setup to measure high-resolution inelastic x-ray scattering at the High Energy Density scientific instrument at the European X-Ray Free-Electron Laser (XFEL). The setup uses the Si (533) reflection in a channel-cut monochromator and three spherical diced analyzer crystals in near-backscattering geometry to reach a high spectral resolution. An energy resolution of 44 meV is demonstrated for the experimental setup, close to the theoretically achievable minimum resolution. The analyzer crystals and detector are mounted on a curved-rail system, allowing quick and reliable changes in scattering angle without breaking vacuum. The entire setup is designed for operation at 10 Hz, the same repetition rate as the high-power lasers available at the instrument and the fundamental repetition rate of the European XFEL. Among other measurements, it is envisioned that this setup will allow studies of the dynamics of highly transient laser generated states of matter.

Original language	English
Article number	013101
Number of pages	9
Journal	Review of Scientific Instruments
Volume	92
Issue number	1
DOIs	https://doi.org/10.1063/5.0022886
Publication status	Published - 04 Jan 2021

Bibliographical note

Funding Information:
We acknowledge the European XFEL in Schenefeld, Germany, for provision of x-ray free-electron laser beamtime at the Scientific Instrument HED (High Energy Density Science) and would like to thank the staff for their assistance. The authors are indebted to the HIBEF user consortium for the provision of instrumentation and staff that enabled this experiment. K.A., T.T., and R.R. acknowledge support from the DFG (Grant No. FOR 2440). Z.K. and C.P. acknowledge support from the DFG Project KO-5262/1. A.D. acknowledges funding from the National Science Foundation under Grant No. 163270. We further acknowledge that this work was supported by the Department of Energy, Laboratory Directed Research and Development program at the SLAC National Accelerator Laboratory under Contract No. DE-AC02-76SF00515 and as part of the Panofsky Fellowship awarded to E.E.M. Furthermore, J.S.W. acknowledges support from the UK EPSRC under Grant No. EP/S025065/1. O.S.H. and O.K. acknowledge support from the Oxford Centre for High Energy Density Science (OxCHEDS). This material is partially based on the work supported by the U.S. Department of Energy, Office of Science, Office of Fusion Energy Science under Award No. DE-SC0019268.

Publisher Copyright:
© 2021 Author(s).

Copyright:
Copyright 2021 Elsevier B.V., All rights reserved.

ASJC Scopus subject areas

Instrumentation

Access to Document

10.1063/5.0022886Licence: CC BY

High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser
Copyright 2021 the authors. This is an open access article published under a Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium, provided the author and source are cited.
Final published version, 3.22 MBLicence: CC BY

26 Citations
2 Comment/debate

Erratum: High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser (Review of Scientific Instruments (2021) 92 (013101) DOI: 10.1063/5.0022886)
Wollenweber, L., Preston, T. R., Descamps, A., Cerantola, V., Comley, A., Eggert, J. H., Fletcher, L. B., Geloni, G., Gericke, D. O., Glenzer, S. H., Göde, S., Hastings, J., Humphries, O. S., Jenei, A., Karnbach, O., Konopkova, Z., Loetzsch, R., Marx-Glowna, B., Mcbride, E. E. & Mcgonegle, D. & 14 others, Monaco, G., Ofori-Okai, B. K., Palmer, C. A. J., Plückthun, C., Redmer, R., Strohm, C., Thorpe, I., Tschentscher, T., Uschmann, I., Wark, J. S., White, T. G., Appel, K., Gregori, G. & Zastrau, U., 16 Mar 2021, In: Review of Scientific Instruments. 92, 3, 0399011.
Research output: Contribution to journal › Comment/debate › peer-review
Publisher’s Note: “High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser” [Rev. Sci. Instrum. 92, 013101 (2021)]
Wollenweber, L., Preston, T. R., Descamps, A., Cerantola, V., Comley, A., Eggert, J. H., Fletcher, L. B., Geloni, G., Gericke, D. O., Glenzer, S. H., Goede, S., Humphries, O. S., Jenei, A., Karnbach, O., Konopkova, Z., Loetzsch, R., Marx-Glowna, B., McBride, E. E., McGonegle, D. & Monaco, G. & 12 others, Ofori-Okai, B. K., Palmer, C. A. J., Plueckthun, C., Redmer, R., Strohm, C., Thorpe, I., Tschentscher, T., Uschmann, I., Wark, J. S., Appel, K., Gregori, G. & Zastrau, U., 16 Mar 2021, In: Review of Scientific Instruments. 92, 3, 039901.
Research output: Contribution to journal › Comment/debate › peer-review

Open Access
File

29 Downloads (Pure)

Cite this

Wollenweber, L., Preston, T. R., Descamps, A., Cerantola, V., Comley, A., Eggert, J. H., Fletcher, L. B., Geloni, G., Gericke, D. O., Glenzer, S. H., Göde, S., Hastings, J., Humphries, O. S., Jenei, A., Karnbach, O., Konopkova, Z., Loetzsch, R., Marx-Glowna, B., McBride, E. E., ... Zastrau, U. (2021). High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser. Review of Scientific Instruments, 92(1), Article 013101. https://doi.org/10.1063/5.0022886

@article{458ab1df0c234348871b286bcbf7f6b6,

title = "High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser",

abstract = "We introduce a setup to measure high-resolution inelastic x-ray scattering at the High Energy Density scientific instrument at the European X-Ray Free-Electron Laser (XFEL). The setup uses the Si (533) reflection in a channel-cut monochromator and three spherical diced analyzer crystals in near-backscattering geometry to reach a high spectral resolution. An energy resolution of 44 meV is demonstrated for the experimental setup, close to the theoretically achievable minimum resolution. The analyzer crystals and detector are mounted on a curved-rail system, allowing quick and reliable changes in scattering angle without breaking vacuum. The entire setup is designed for operation at 10 Hz, the same repetition rate as the high-power lasers available at the instrument and the fundamental repetition rate of the European XFEL. Among other measurements, it is envisioned that this setup will allow studies of the dynamics of highly transient laser generated states of matter. ",

author = "L. Wollenweber and Preston, {T. R.} and A. Descamps and V. Cerantola and A. Comley and Eggert, {J. H.} and Fletcher, {L. B.} and G. Geloni and Gericke, {D. O.} and Glenzer, {S. H.} and S. G{\"o}de and J. Hastings and Humphries, {O. S.} and A. Jenei and O. Karnbach and Z. Konopkova and R. Loetzsch and B. Marx-Glowna and McBride, {E. E.} and D. McGonegle and G. Monaco and Ofori-Okai, {B. K.} and Palmer, {C. A.J.} and C. Pl{\"u}ckthun and R. Redmer and C. Strohm and I. Thorpe and T. Tschentscher and I. Uschmann and Wark, {J. S.} and White, {T. G.} and K. Appel and G. Gregori and U. Zastrau",

note = "Funding Information: We acknowledge the European XFEL in Schenefeld, Germany, for provision of x-ray free-electron laser beamtime at the Scientific Instrument HED (High Energy Density Science) and would like to thank the staff for their assistance. The authors are indebted to the HIBEF user consortium for the provision of instrumentation and staff that enabled this experiment. K.A., T.T., and R.R. acknowledge support from the DFG (Grant No. FOR 2440). Z.K. and C.P. acknowledge support from the DFG Project KO-5262/1. A.D. acknowledges funding from the National Science Foundation under Grant No. 163270. We further acknowledge that this work was supported by the Department of Energy, Laboratory Directed Research and Development program at the SLAC National Accelerator Laboratory under Contract No. DE-AC02-76SF00515 and as part of the Panofsky Fellowship awarded to E.E.M. Furthermore, J.S.W. acknowledges support from the UK EPSRC under Grant No. EP/S025065/1. O.S.H. and O.K. acknowledge support from the Oxford Centre for High Energy Density Science (OxCHEDS). This material is partially based on the work supported by the U.S. Department of Energy, Office of Science, Office of Fusion Energy Science under Award No. DE-SC0019268. Publisher Copyright: {\textcopyright} 2021 Author(s). Copyright: Copyright 2021 Elsevier B.V., All rights reserved.",

year = "2021",

month = jan,

day = "4",

doi = "10.1063/5.0022886",

language = "English",

volume = "92",

journal = "Review of Scientific Instruments",

issn = "0034-6748",

publisher = "American Institute of Physics",

number = "1",

}

Wollenweber, L, Preston, TR, Descamps, A, Cerantola, V, Comley, A, Eggert, JH, Fletcher, LB, Geloni, G, Gericke, DO, Glenzer, SH, Göde, S, Hastings, J, Humphries, OS, Jenei, A, Karnbach, O, Konopkova, Z, Loetzsch, R, Marx-Glowna, B, McBride, EE, McGonegle, D, Monaco, G, Ofori-Okai, BK, Palmer, CAJ, Plückthun, C, Redmer, R, Strohm, C, Thorpe, I, Tschentscher, T, Uschmann, I, Wark, JS, White, TG, Appel, K, Gregori, G & Zastrau, U 2021, 'High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser', Review of Scientific Instruments, vol. 92, no. 1, 013101. https://doi.org/10.1063/5.0022886

TY - JOUR

T1 - High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser

AU - Wollenweber, L.

AU - Preston, T. R.

AU - Descamps, A.

AU - Cerantola, V.

AU - Comley, A.

AU - Eggert, J. H.

AU - Fletcher, L. B.

AU - Geloni, G.

AU - Gericke, D. O.

AU - Glenzer, S. H.

AU - Göde, S.

AU - Hastings, J.

AU - Humphries, O. S.

AU - Jenei, A.

AU - Karnbach, O.

AU - Konopkova, Z.

AU - Loetzsch, R.

AU - Marx-Glowna, B.

AU - McBride, E. E.

AU - McGonegle, D.

AU - Monaco, G.

AU - Ofori-Okai, B. K.

AU - Palmer, C. A.J.

AU - Plückthun, C.

AU - Redmer, R.

AU - Strohm, C.

AU - Thorpe, I.

AU - Tschentscher, T.

AU - Uschmann, I.

AU - Wark, J. S.

AU - White, T. G.

AU - Appel, K.

AU - Gregori, G.

AU - Zastrau, U.

N1 - Funding Information: We acknowledge the European XFEL in Schenefeld, Germany, for provision of x-ray free-electron laser beamtime at the Scientific Instrument HED (High Energy Density Science) and would like to thank the staff for their assistance. The authors are indebted to the HIBEF user consortium for the provision of instrumentation and staff that enabled this experiment. K.A., T.T., and R.R. acknowledge support from the DFG (Grant No. FOR 2440). Z.K. and C.P. acknowledge support from the DFG Project KO-5262/1. A.D. acknowledges funding from the National Science Foundation under Grant No. 163270. We further acknowledge that this work was supported by the Department of Energy, Laboratory Directed Research and Development program at the SLAC National Accelerator Laboratory under Contract No. DE-AC02-76SF00515 and as part of the Panofsky Fellowship awarded to E.E.M. Furthermore, J.S.W. acknowledges support from the UK EPSRC under Grant No. EP/S025065/1. O.S.H. and O.K. acknowledge support from the Oxford Centre for High Energy Density Science (OxCHEDS). This material is partially based on the work supported by the U.S. Department of Energy, Office of Science, Office of Fusion Energy Science under Award No. DE-SC0019268. Publisher Copyright: © 2021 Author(s). Copyright: Copyright 2021 Elsevier B.V., All rights reserved.

PY - 2021/1/4

Y1 - 2021/1/4

N2 - We introduce a setup to measure high-resolution inelastic x-ray scattering at the High Energy Density scientific instrument at the European X-Ray Free-Electron Laser (XFEL). The setup uses the Si (533) reflection in a channel-cut monochromator and three spherical diced analyzer crystals in near-backscattering geometry to reach a high spectral resolution. An energy resolution of 44 meV is demonstrated for the experimental setup, close to the theoretically achievable minimum resolution. The analyzer crystals and detector are mounted on a curved-rail system, allowing quick and reliable changes in scattering angle without breaking vacuum. The entire setup is designed for operation at 10 Hz, the same repetition rate as the high-power lasers available at the instrument and the fundamental repetition rate of the European XFEL. Among other measurements, it is envisioned that this setup will allow studies of the dynamics of highly transient laser generated states of matter.

AB - We introduce a setup to measure high-resolution inelastic x-ray scattering at the High Energy Density scientific instrument at the European X-Ray Free-Electron Laser (XFEL). The setup uses the Si (533) reflection in a channel-cut monochromator and three spherical diced analyzer crystals in near-backscattering geometry to reach a high spectral resolution. An energy resolution of 44 meV is demonstrated for the experimental setup, close to the theoretically achievable minimum resolution. The analyzer crystals and detector are mounted on a curved-rail system, allowing quick and reliable changes in scattering angle without breaking vacuum. The entire setup is designed for operation at 10 Hz, the same repetition rate as the high-power lasers available at the instrument and the fundamental repetition rate of the European XFEL. Among other measurements, it is envisioned that this setup will allow studies of the dynamics of highly transient laser generated states of matter.

U2 - 10.1063/5.0022886

DO - 10.1063/5.0022886

M3 - Article

C2 - 33514249

AN - SCOPUS:85099522607

SN - 0034-6748

VL - 92

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

IS - 1

M1 - 013101

ER -

High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser

Abstract

Bibliographical note

ASJC Scopus subject areas

Access to Document

Fingerprint

Research output

Erratum: High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser (Review of Scientific Instruments (2021) 92 (013101) DOI: 10.1063/5.0022886)

Publisher’s Note: “High-resolution inelastic x-ray scattering at the high energy density scientific instrument at the European X-Ray Free-Electron Laser” [Rev. Sci. Instrum. 92, 013101 (2021)]

Cite this