In-Situ, Simultaneous Irradiation and Monitoring of a Photocatalysed Organic Oxidation Reaction in a TiO2-coated NMR Tube

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Abstract

The semiconductor photocatalysed (SPC) oxidation of toluene is performed inside an NMR spectrometer and the reaction monitored simultaneously in-situ, using a fibre optic probe/diffuser to provide the UV light to activate the titania photocatalyst coating on the inside of the NMR tube. Such a system has great potential for the simple rapid screening of a wide range of SPC mediated organic reactions.
Original languageEnglish
Pages (from-to)10342-10345
Number of pages4
JournalJournal of Organic Chemistry
Volume80
Issue number20
Early online date28 Sep 2015
DOIs
Publication statusPublished - 2015

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