Microwave-assisted synthesis of Limonia acidissima Groff gum stabilized palladium nanoparticles for colorimetric glucose sensing

Kondaiah Seku, Babu Pejjai, Ahmed I. Osman*, Syed Sulaiman Hussaini, Mohammed Al-Abri, R. Swathi, Mushtaq Hussain, Nadavala Siva Kumar, Ahmed S. Al-Fatesh, G. Bhagavanth Reddy*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

2 Citations (Scopus)
27 Downloads (Pure)

Abstract

Herein, we present a novel microwave-assisted method for the synthesis of palladium nanoparticles (PdNPs) supported by Limonia acidissima Groff tree extract gum. The synthesized PdNPs were characterized using various analytical techniques, including FTIR, SEM, TEM, UV–visible, and powder XRD analyses. TEM and XRD analysis confirmed that the synthesized LAG-PdNPs are highly crystalline nature spherical shapes with an average size diameter of 7–9 nm. We employed these gum-capped PdNPs to investigate their peroxidase-like activity for colorimetric detection of hydrogen peroxide (H2O2) and glucose. The oxidation of 3,3′,5,5′-tetramethylbenzidine (TMB) by H2O2, catalyzed by PdNPs, produces oxidation products quantified at 652 nm using spectrophotometry. The catalytic activity of PdNPs was optimized with respect to temperature and pH. The developed method exhibited a linear range of detection from 1 to 50 µm, with detection limits of 0.35 µm for H2O2 and 0.60 µm for glucose.

Original languageEnglish
Pages (from-to)718-727
Number of pages10
JournalJournal of Colloid and Interface Science
Volume659
Early online date11 Jan 2024
DOIs
Publication statusPublished - Apr 2024

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