Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

H. P. Liermann; Z. Konopkova; K. Appel; C. Prescher; A. Schropp; V. Cerantola; R. J. Husband; J. D. McHardy; M. I. McMahon; R. S. McWilliams; C. M. Pepin; J. Mainberger; M. Roeper; A. Berghauser; H. Damker; P. Talkovski; M. Foese; N. Kujala; O. B. Ball; M. A. Baron; R. Briggs; M. Bykov; E. Bykova; J. Chantel; A. L. Coleman; H. Cynn; D. Dattelbaum; L. E. Dresselhaus-Marais; J. H. Eggert; L. Ehm; W. J. Evans; G. Fiquet; M. Frost; K. Glazyrin; A. F. Goncharov; H. Hwang; Zs Jenei; J. Y. Kim; F. Langenhorst; Y. Lee; M. Makita; H. Marquardt; E. E. McBride; S. Merkel; G. Morard; E. F. O'Bannon; C. Otzen; E. J. Pace; A. Pelka; J. S. Pigott; V. B. Prakapenka; R. Redmer; C. Sanchez-Valle; M. Schoelmerich; S. Speziale; G. Spiekermann; B. T. Sturtevant; S. Toleikis; N. Velisavljevic; M. Wilke; C. S. Yoo; C. Baehtz; U. Zastrau; C. Strohm

doi:10.1107/s1600577521002551

Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

H. P. Liermann^*, Z. Konopkova, K. Appel, C. Prescher, A. Schropp, V. Cerantola, R. J. Husband, J. D. McHardy, M. I. McMahon, R. S. McWilliams, C. M. Pepin, J. Mainberger, M. Roeper, A. Berghauser, H. Damker, P. Talkovski, M. Foese, N. Kujala, O. B. Ball, M. A. BaronR. Briggs, M. Bykov, E. Bykova, J. Chantel, A. L. Coleman, H. Cynn, D. Dattelbaum, L. E. Dresselhaus-Marais, J. H. Eggert, L. Ehm, W. J. Evans, G. Fiquet, M. Frost, K. Glazyrin, A. F. Goncharov, H. Hwang, Zs Jenei, J. Y. Kim, F. Langenhorst, Y. Lee, M. Makita, H. Marquardt, E. E. McBride, S. Merkel, G. Morard, E. F. O'Bannon, C. Otzen, E. J. Pace, A. Pelka, J. S. Pigott, V. B. Prakapenka, R. Redmer, C. Sanchez-Valle, M. Schoelmerich, S. Speziale, G. Spiekermann, B. T. Sturtevant, S. Toleikis, N. Velisavljevic, M. Wilke, C. S. Yoo, C. Baehtz, U. Zastrau, C. Strohm

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

27 Citations (Scopus)

42 Downloads (Pure)

Abstract

The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

Original language	English
Pages (from-to)	688-706
Number of pages	19
Journal	Journal of Synchrotron Radiation
Volume	28
Issue number	3
DOIs	https://doi.org/10.1107/s1600577521002551
Publication status	Published - 01 May 2021
Externally published	Yes

Bibliographical note

Funding Information:
The research leading to these results has been supported by the project CALIPSOplus under Grant Agreement 730872 from the EU Framework Programme for Research and Innovation HORIZON 2020. KA, MaF, KG, RJH, ZK, HPL, RR, CSV and MS thank the DFG for support within the Research Unit FOR 2440. YL is grateful for support from the Leader Researcher program (NRF-2018R1A3B1052042) of the Korean Ministry of Science and ICT (MSIT). Part of this work was performed under the auspices of the US Department of Energy by Lawrence Livermore National Laboratory under Contract No. DE-AC52-07NA27344, and by the US Department of Energy through the Los Alamos National Laboratory, operated by Triad National Security LLC for the National Nuclear Security Administration (Contract No. 89233218CNA000001). Research presented in this article was supported by the US Department of Energy Laboratory Directed Research and Development program at Los Alamos National Laboratory under project No. 20190643DR and at SLAC National Accelerator Laboratory under contract DE-AC02-76SF00515. Support is acknowledged from the Panofsky Fellowship at SLAC (awarded to EEM), the DOE Office of Fusion Energy Science funding No. FWP100182 (MF and EEM), EPSRC Grants EP/P024513/1 (RSM) and EP/ R02927X/1 (EJP and MIM), and the European Research Council (ERC) under the European Union’s Horizon 2020 Research and Innovation Programme for grant agreements Nos. 670787 (GF, MAB, and GM) and 864877 (HM). SM and JC acknowledge support from the I-SITE ULNE project MetalCore (R-ERCGEN-19-006-MERKEL). CSY acknowledges the US DOE-NNSA (DE-NA0003342), National Science Foundation (DMR-1701360) and Army Research Office (W911NF-17-1-0468). MB and AFG acknowledge support from the Army Research Office under Cooperative Agreement No. W911NF-19-2-0172. VBP acknowledge support from the National Science Foundation – Earth Sciences (EAR-1634415).

Publisher Copyright:
© 2021 International Union of Crystallography. All rights reserved.

Keywords

Diamond anvil cells
Finite element modeling
High-precision X-ray diffraction
X-ray free-electron lasers

ASJC Scopus subject areas

Radiation
Nuclear and High Energy Physics
Instrumentation

Access to Document

10.1107/s1600577521002551Licence: CC BY

Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)
Copyright 2022 the authors. This is an open access article published under a Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium, provided the author and source are cited.
Final published version, 2.46 MBLicence: CC BY

Cite this

Liermann, H. P., Konopkova, Z., Appel, K., Prescher, C., Schropp, A., Cerantola, V., Husband, R. J., McHardy, J. D., McMahon, M. I., McWilliams, R. S., Pepin, C. M., Mainberger, J., Roeper, M., Berghauser, A., Damker, H., Talkovski, P., Foese, M., Kujala, N., Ball, O. B., ... Strohm, C. (2021). Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL). Journal of Synchrotron Radiation, 28(3), 688-706. https://doi.org/10.1107/s1600577521002551

@article{14a8a9dfa99d493cb124619d53379926,

title = "Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)",

abstract = "The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.",

keywords = "Diamond anvil cells, Finite element modeling, High-precision X-ray diffraction, X-ray free-electron lasers",

author = "Liermann, {H. P.} and Z. Konopkova and K. Appel and C. Prescher and A. Schropp and V. Cerantola and Husband, {R. J.} and McHardy, {J. D.} and McMahon, {M. I.} and McWilliams, {R. S.} and Pepin, {C. M.} and J. Mainberger and M. Roeper and A. Berghauser and H. Damker and P. Talkovski and M. Foese and N. Kujala and Ball, {O. B.} and Baron, {M. A.} and R. Briggs and M. Bykov and E. Bykova and J. Chantel and Coleman, {A. L.} and H. Cynn and D. Dattelbaum and Dresselhaus-Marais, {L. E.} and Eggert, {J. H.} and L. Ehm and Evans, {W. J.} and G. Fiquet and M. Frost and K. Glazyrin and Goncharov, {A. F.} and H. Hwang and Zs Jenei and Kim, {J. Y.} and F. Langenhorst and Y. Lee and M. Makita and H. Marquardt and McBride, {E. E.} and S. Merkel and G. Morard and O'Bannon, {E. F.} and C. Otzen and Pace, {E. J.} and A. Pelka and Pigott, {J. S.} and Prakapenka, {V. B.} and R. Redmer and C. Sanchez-Valle and M. Schoelmerich and S. Speziale and G. Spiekermann and Sturtevant, {B. T.} and S. Toleikis and N. Velisavljevic and M. Wilke and Yoo, {C. S.} and C. Baehtz and U. Zastrau and C. Strohm",

note = "Funding Information: The research leading to these results has been supported by the project CALIPSOplus under Grant Agreement 730872 from the EU Framework Programme for Research and Innovation HORIZON 2020. KA, MaF, KG, RJH, ZK, HPL, RR, CSV and MS thank the DFG for support within the Research Unit FOR 2440. YL is grateful for support from the Leader Researcher program (NRF-2018R1A3B1052042) of the Korean Ministry of Science and ICT (MSIT). Part of this work was performed under the auspices of the US Department of Energy by Lawrence Livermore National Laboratory under Contract No. DE-AC52-07NA27344, and by the US Department of Energy through the Los Alamos National Laboratory, operated by Triad National Security LLC for the National Nuclear Security Administration (Contract No. 89233218CNA000001). Research presented in this article was supported by the US Department of Energy Laboratory Directed Research and Development program at Los Alamos National Laboratory under project No. 20190643DR and at SLAC National Accelerator Laboratory under contract DE-AC02-76SF00515. Support is acknowledged from the Panofsky Fellowship at SLAC (awarded to EEM), the DOE Office of Fusion Energy Science funding No. FWP100182 (MF and EEM), EPSRC Grants EP/P024513/1 (RSM) and EP/ R02927X/1 (EJP and MIM), and the European Research Council (ERC) under the European Union{\textquoteright}s Horizon 2020 Research and Innovation Programme for grant agreements Nos. 670787 (GF, MAB, and GM) and 864877 (HM). SM and JC acknowledge support from the I-SITE ULNE project MetalCore (R-ERCGEN-19-006-MERKEL). CSY acknowledges the US DOE-NNSA (DE-NA0003342), National Science Foundation (DMR-1701360) and Army Research Office (W911NF-17-1-0468). MB and AFG acknowledge support from the Army Research Office under Cooperative Agreement No. W911NF-19-2-0172. VBP acknowledge support from the National Science Foundation – Earth Sciences (EAR-1634415). Publisher Copyright: {\textcopyright} 2021 International Union of Crystallography. All rights reserved.",

year = "2021",

month = may,

day = "1",

doi = "10.1107/s1600577521002551",

language = "English",

volume = "28",

pages = "688--706",

journal = "Journal of Synchrotron Radiation",

issn = "1600-5775",

publisher = "International Union of Crystallography",

number = "3",

}

Liermann, HP, Konopkova, Z, Appel, K, Prescher, C, Schropp, A, Cerantola, V, Husband, RJ, McHardy, JD, McMahon, MI, McWilliams, RS, Pepin, CM, Mainberger, J, Roeper, M, Berghauser, A, Damker, H, Talkovski, P, Foese, M, Kujala, N, Ball, OB, Baron, MA, Briggs, R, Bykov, M, Bykova, E, Chantel, J, Coleman, AL, Cynn, H, Dattelbaum, D, Dresselhaus-Marais, LE, Eggert, JH, Ehm, L, Evans, WJ, Fiquet, G, Frost, M, Glazyrin, K, Goncharov, AF, Hwang, H, Jenei, Z, Kim, JY, Langenhorst, F, Lee, Y, Makita, M, Marquardt, H, McBride, EE, Merkel, S, Morard, G, O'Bannon, EF, Otzen, C, Pace, EJ, Pelka, A, Pigott, JS, Prakapenka, VB, Redmer, R, Sanchez-Valle, C, Schoelmerich, M, Speziale, S, Spiekermann, G, Sturtevant, BT, Toleikis, S, Velisavljevic, N, Wilke, M, Yoo, CS, Baehtz, C, Zastrau, U & Strohm, C 2021, 'Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)', Journal of Synchrotron Radiation, vol. 28, no. 3, pp. 688-706. https://doi.org/10.1107/s1600577521002551

Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL). / Liermann, H. P.; Konopkova, Z.; Appel, K. et al.
In: Journal of Synchrotron Radiation, Vol. 28, No. 3, 01.05.2021, p. 688-706.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

AU - Liermann, H. P.

AU - Konopkova, Z.

AU - Appel, K.

AU - Prescher, C.

AU - Schropp, A.

AU - Cerantola, V.

AU - Husband, R. J.

AU - McHardy, J. D.

AU - McMahon, M. I.

AU - McWilliams, R. S.

AU - Pepin, C. M.

AU - Mainberger, J.

AU - Roeper, M.

AU - Berghauser, A.

AU - Damker, H.

AU - Talkovski, P.

AU - Foese, M.

AU - Kujala, N.

AU - Ball, O. B.

AU - Baron, M. A.

AU - Briggs, R.

AU - Bykov, M.

AU - Bykova, E.

AU - Chantel, J.

AU - Coleman, A. L.

AU - Cynn, H.

AU - Dattelbaum, D.

AU - Dresselhaus-Marais, L. E.

AU - Eggert, J. H.

AU - Ehm, L.

AU - Evans, W. J.

AU - Fiquet, G.

AU - Frost, M.

AU - Glazyrin, K.

AU - Goncharov, A. F.

AU - Hwang, H.

AU - Jenei, Zs

AU - Kim, J. Y.

AU - Langenhorst, F.

AU - Lee, Y.

AU - Makita, M.

AU - Marquardt, H.

AU - McBride, E. E.

AU - Merkel, S.

AU - Morard, G.

AU - O'Bannon, E. F.

AU - Otzen, C.

AU - Pace, E. J.

AU - Pelka, A.

AU - Pigott, J. S.

AU - Prakapenka, V. B.

AU - Redmer, R.

AU - Sanchez-Valle, C.

AU - Schoelmerich, M.

AU - Speziale, S.

AU - Spiekermann, G.

AU - Sturtevant, B. T.

AU - Toleikis, S.

AU - Velisavljevic, N.

AU - Wilke, M.

AU - Yoo, C. S.

AU - Baehtz, C.

AU - Zastrau, U.

AU - Strohm, C.

N1 - Funding Information: The research leading to these results has been supported by the project CALIPSOplus under Grant Agreement 730872 from the EU Framework Programme for Research and Innovation HORIZON 2020. KA, MaF, KG, RJH, ZK, HPL, RR, CSV and MS thank the DFG for support within the Research Unit FOR 2440. YL is grateful for support from the Leader Researcher program (NRF-2018R1A3B1052042) of the Korean Ministry of Science and ICT (MSIT). Part of this work was performed under the auspices of the US Department of Energy by Lawrence Livermore National Laboratory under Contract No. DE-AC52-07NA27344, and by the US Department of Energy through the Los Alamos National Laboratory, operated by Triad National Security LLC for the National Nuclear Security Administration (Contract No. 89233218CNA000001). Research presented in this article was supported by the US Department of Energy Laboratory Directed Research and Development program at Los Alamos National Laboratory under project No. 20190643DR and at SLAC National Accelerator Laboratory under contract DE-AC02-76SF00515. Support is acknowledged from the Panofsky Fellowship at SLAC (awarded to EEM), the DOE Office of Fusion Energy Science funding No. FWP100182 (MF and EEM), EPSRC Grants EP/P024513/1 (RSM) and EP/ R02927X/1 (EJP and MIM), and the European Research Council (ERC) under the European Union’s Horizon 2020 Research and Innovation Programme for grant agreements Nos. 670787 (GF, MAB, and GM) and 864877 (HM). SM and JC acknowledge support from the I-SITE ULNE project MetalCore (R-ERCGEN-19-006-MERKEL). CSY acknowledges the US DOE-NNSA (DE-NA0003342), National Science Foundation (DMR-1701360) and Army Research Office (W911NF-17-1-0468). MB and AFG acknowledge support from the Army Research Office under Cooperative Agreement No. W911NF-19-2-0172. VBP acknowledge support from the National Science Foundation – Earth Sciences (EAR-1634415). Publisher Copyright: © 2021 International Union of Crystallography. All rights reserved.

PY - 2021/5/1

Y1 - 2021/5/1

N2 - The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

AB - The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump–probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

KW - Diamond anvil cells

KW - Finite element modeling

KW - High-precision X-ray diffraction

KW - X-ray free-electron lasers

U2 - 10.1107/s1600577521002551

DO - 10.1107/s1600577521002551

M3 - Article

C2 - 33949979

SN - 1600-5775

VL - 28

SP - 688

EP - 706

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

IS - 3

ER -

Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

Access to Document

Fingerprint

Cite this