Overcoming the solvation shell during the crystallisation of diatrizoic acid from dimethylsulfoxide.

Katharina Edkins; Judith A.K. Howard; Jonathan W. Steed

doi:10.1039/c2cc35995b

Overcoming the solvation shell during the crystallisation of diatrizoic acid from dimethylsulfoxide.

Katharina Edkins, Judith A.K. Howard, Jonathan W. Steed

School of Pharmacy

Research output: Contribution to journal › Article › peer-review

12 Citations (Scopus)

Abstract

We present three crystal structures of diatrizoic acid (DTA) DMSO solvates illustrating progressive desolvation of the DTA molecule and concomitant increasing degree of DTA self-association. Using these structures, plausible pathways for overcoming the solvation shell of DTA during its crystallisation from solution are discussed.

Original language	English
Pages (from-to)	12065-12067
Number of pages	3
Journal	Chemical Communications
Volume	48
Issue number	99
DOIs	https://doi.org/10.1039/c2cc35995b
Publication status	Published - 26 Oct 2012

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title = "Overcoming the solvation shell during the crystallisation of diatrizoic acid from dimethylsulfoxide.",

abstract = "We present three crystal structures of diatrizoic acid (DTA) DMSO solvates illustrating progressive desolvation of the DTA molecule and concomitant increasing degree of DTA self-association. Using these structures, plausible pathways for overcoming the solvation shell of DTA during its crystallisation from solution are discussed.",

author = "Katharina Edkins and Howard, {Judith A.K.} and Steed, {Jonathan W.}",

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T1 - Overcoming the solvation shell during the crystallisation of diatrizoic acid from dimethylsulfoxide.

AU - Edkins, Katharina

AU - Howard, Judith A.K.

AU - Steed, Jonathan W.

PY - 2012/10/26

Y1 - 2012/10/26

N2 - We present three crystal structures of diatrizoic acid (DTA) DMSO solvates illustrating progressive desolvation of the DTA molecule and concomitant increasing degree of DTA self-association. Using these structures, plausible pathways for overcoming the solvation shell of DTA during its crystallisation from solution are discussed.

AB - We present three crystal structures of diatrizoic acid (DTA) DMSO solvates illustrating progressive desolvation of the DTA molecule and concomitant increasing degree of DTA self-association. Using these structures, plausible pathways for overcoming the solvation shell of DTA during its crystallisation from solution are discussed.

U2 - 10.1039/c2cc35995b

DO - 10.1039/c2cc35995b

M3 - Article

SN - 1359-7345

VL - 48

SP - 12065

EP - 12067

JO - Chemical Communications

JF - Chemical Communications

IS - 99

ER -

Overcoming the solvation shell during the crystallisation of diatrizoic acid from dimethylsulfoxide.

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