Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing

Sabitha Ann Jose; Yahya Atwa; Neil Mitchell; Hamza Shakeel

doi:10.1109/APSCON56343.2023.10101020

Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing

Sabitha Ann Jose, Yahya Atwa, Neil Mitchell, Hamza Shakeel

School of Electronics, Electrical Engineering and Computer Science

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

In this study, we demonstrate a graphene-based portable gas sensor with an integrated fused silica micro chamber for direct on-chip sample injection to detect a low concentration (∼10 ppm) of acetone from a soil sample at room temperature and pressure. A chemiresistive gas sensor was first fabricated by a conformal transfer process using a commercial monolayer graphene film. Printable fused silica micro gas chamber (internal volume of 50 microliter), fabricated separately, was permanently attached with the graphene chemiresistor using an ultra-violet light source. A relative resistance change of 1% (∼20 ppm of acetone) was achieved by injection of a headspace sample for acetone calibration. This direct on-chip injection method shows an excellent potential for detecting volatile organic compounds from a soil sample without requiring complex sample extraction steps.

Original language	English
Title of host publication	Proceedings of the IEEE Applied Sensing Conference, APSCON 2023
Publisher	Institute of Electrical and Electronics Engineers Inc.
Number of pages	3
ISBN (Electronic)	9781665461634
ISBN (Print)	9781665461641
DOIs	https://doi.org/10.1109/APSCON56343.2023.10101020
Publication status	Published - 17 Apr 2023
Event	IEEE Applied Sensing Conference 2023 - Bengaluru, India Duration: 23 Jan 2023 → 25 Apr 2023

Publication series

Name	IEEE Applied Sensing Conference (APSCON): Proceedings

Conference

Conference	IEEE Applied Sensing Conference 2023
Abbreviated title	APSCON 2023
Country/Territory	India
City	Bengaluru
Period	23/01/2023 → 25/04/2023

Keywords

graphene chemi-resistor ,
soil testing
Direct injection vapor sensing
Printable glass chamber

Access to Document

10.1109/APSCON56343.2023.10101020Licence: Unspecified

1 Finished

R3201ECI: EPMD: Enabling next generation integrated optoelectronics with free-form metamaterials based on graphene
Shakeel, H. (PI)
21/01/2020 → 30/11/2023
Project: Research

Design and fabrication of highly sensitive graphene-based sensors for environmental and health monitoring applications
Ann Jose, S. (Author), McNeill, D. (Supervisor) & Shakeel, H. (Supervisor), Jul 2024
Student thesis: Doctoral Thesis › Doctor of Philosophy

File

1 Conference contribution
1 Article

Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing
Ann Jose, S., Atwa, Y., Mitchell, N. & Shakeel, H., 17 Apr 2023, Proceedings of the IEEE Applied Sensing Conference, APSCON 2023. Institute of Electrical and Electronics Engineers Inc., 3 p. (IEEE Applied Sensing Conference (APSCON): Proceedings).
Research output: Chapter in Book/Report/Conference proceeding › Conference contribution
Restoring adsorption properties of graphene sensor with printable glass encapsulation using UV illumination
Ann Jose, S., Atwa, Y., Mao, J. & Shakeel, H., Jul 2023, In: Flatchem. 40, 8 p., 100510.
Research output: Contribution to journal › Article › peer-review

Open Access
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4 Citations (Scopus)

37 Downloads (Pure)

Cite this

Ann Jose, S., Atwa, Y., Mitchell, N., & Shakeel, H. (2023). Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing. In Proceedings of the IEEE Applied Sensing Conference, APSCON 2023 (IEEE Applied Sensing Conference (APSCON): Proceedings). Institute of Electrical and Electronics Engineers Inc.. https://doi.org/10.1109/APSCON56343.2023.10101020

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title = "Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing",

abstract = "In this study, we demonstrate a graphene-based portable gas sensor with an integrated fused silica micro chamber for direct on-chip sample injection to detect a low concentration (∼10 ppm) of acetone from a soil sample at room temperature and pressure. A chemiresistive gas sensor was first fabricated by a conformal transfer process using a commercial monolayer graphene film. Printable fused silica micro gas chamber (internal volume of 50 microliter), fabricated separately, was permanently attached with the graphene chemiresistor using an ultra-violet light source. A relative resistance change of 1% (∼20 ppm of acetone) was achieved by injection of a headspace sample for acetone calibration. This direct on-chip injection method shows an excellent potential for detecting volatile organic compounds from a soil sample without requiring complex sample extraction steps.",

keywords = "graphene chemi-resistor ,, soil testing, Direct injection vapor sensing, Printable glass chamber",

author = "{Ann Jose}, Sabitha and Yahya Atwa and Neil Mitchell and Hamza Shakeel",

year = "2023",

month = apr,

day = "17",

doi = "10.1109/APSCON56343.2023.10101020",

language = "English",

isbn = "9781665461641",

series = "IEEE Applied Sensing Conference (APSCON): Proceedings",

publisher = "Institute of Electrical and Electronics Engineers Inc.",

booktitle = "Proceedings of the IEEE Applied Sensing Conference, APSCON 2023",

address = "United States",

note = "IEEE Applied Sensing Conference 2023, APSCON 2023 ; Conference date: 23-01-2023 Through 25-04-2023",

}

Ann Jose, S , Atwa, Y , Mitchell, N & Shakeel, H 2023, Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing. in Proceedings of the IEEE Applied Sensing Conference, APSCON 2023. IEEE Applied Sensing Conference (APSCON): Proceedings, Institute of Electrical and Electronics Engineers Inc., IEEE Applied Sensing Conference 2023, Bengaluru, India, 23/01/2023. https://doi.org/10.1109/APSCON56343.2023.10101020

Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing. / Ann Jose, Sabitha ; Atwa, Yahya ; Mitchell, Neil et al.
Proceedings of the IEEE Applied Sensing Conference, APSCON 2023. Institute of Electrical and Electronics Engineers Inc., 2023. (IEEE Applied Sensing Conference (APSCON): Proceedings).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

TY - GEN

T1 - Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing

AU - Ann Jose, Sabitha

AU - Atwa, Yahya

AU - Mitchell, Neil

AU - Shakeel, Hamza

PY - 2023/4/17

Y1 - 2023/4/17

N2 - In this study, we demonstrate a graphene-based portable gas sensor with an integrated fused silica micro chamber for direct on-chip sample injection to detect a low concentration (∼10 ppm) of acetone from a soil sample at room temperature and pressure. A chemiresistive gas sensor was first fabricated by a conformal transfer process using a commercial monolayer graphene film. Printable fused silica micro gas chamber (internal volume of 50 microliter), fabricated separately, was permanently attached with the graphene chemiresistor using an ultra-violet light source. A relative resistance change of 1% (∼20 ppm of acetone) was achieved by injection of a headspace sample for acetone calibration. This direct on-chip injection method shows an excellent potential for detecting volatile organic compounds from a soil sample without requiring complex sample extraction steps.

AB - In this study, we demonstrate a graphene-based portable gas sensor with an integrated fused silica micro chamber for direct on-chip sample injection to detect a low concentration (∼10 ppm) of acetone from a soil sample at room temperature and pressure. A chemiresistive gas sensor was first fabricated by a conformal transfer process using a commercial monolayer graphene film. Printable fused silica micro gas chamber (internal volume of 50 microliter), fabricated separately, was permanently attached with the graphene chemiresistor using an ultra-violet light source. A relative resistance change of 1% (∼20 ppm of acetone) was achieved by injection of a headspace sample for acetone calibration. This direct on-chip injection method shows an excellent potential for detecting volatile organic compounds from a soil sample without requiring complex sample extraction steps.

KW - graphene chemi-resistor ,

KW - soil testing

KW - Direct injection vapor sensing

KW - Printable glass chamber

U2 - 10.1109/APSCON56343.2023.10101020

DO - 10.1109/APSCON56343.2023.10101020

M3 - Conference contribution

SN - 9781665461641

T3 - IEEE Applied Sensing Conference (APSCON): Proceedings

BT - Proceedings of the IEEE Applied Sensing Conference, APSCON 2023

PB - Institute of Electrical and Electronics Engineers Inc.

T2 - IEEE Applied Sensing Conference 2023

Y2 - 23 January 2023 through 25 April 2023

ER -

Ann Jose S , Atwa Y , Mitchell N , Shakeel H. Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing. In Proceedings of the IEEE Applied Sensing Conference, APSCON 2023. Institute of Electrical and Electronics Engineers Inc. 2023. (IEEE Applied Sensing Conference (APSCON): Proceedings). doi: 10.1109/APSCON56343.2023.10101020

Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing

Abstract

Publication series

Conference

Keywords

Access to Document

Fingerprint

Projects

R3201ECI: EPMD: Enabling next generation integrated optoelectronics with free-form metamaterials based on graphene

Student theses

Design and fabrication of highly sensitive graphene-based sensors for environmental and health monitoring applications

Research output

Printable fused silica based microchamber integrated with graphene chemi-resistive sensors for direct on-chip soil testing

Restoring adsorption properties of graphene sensor with printable glass encapsulation using UV illumination

Cite this